Recent advances in green carbon dots (2015–2022): synthesis, metal ion sensing, and biological applications

• Aisha Kanwal,
• Naheed Bibi,
• Sajjad Hyder,
• Arif Muhammad,
• Hao Ren,
• Jiangtao Liu and
• Zhongli Lei

Beilstein J. Nanotechnol. 2022, 13, 1068–1107, doi:10.3762/bjnano.13.93

• EDA as nitrogen dopant to synthesize N-CDs via one-pot hydrothermal carbonization approach have been used. Three different operating parameters, that is, synthesis temperature (230–270 °C), synthesis time (2–6 h), and EDA mass (10%–23.3%) were studied using response surface methodology. The highest

• the electronic structure of CDs, N,S-CDs have drawn more interest in recent years. Li et al. reported a simple and economical one-pot hydrothermal carbonization route to prepare N,S-CDs by using ginkgo leaves as a natural precursor. XPS results demonstrated that the reported CDs were having elemental

• waste as carbon and nitrogen source, novel CDs have been prepared using a simple hydrothermal carbonization technique in an ecofriendly approach by Atchudan et al. [79]. Their excitation-dependent fluorescence characteristics have been used successfully as a fluorescent probe in multicolor imaging

Gas sorption porosimetry for the evaluation of hard carbons as anodes for Li- and Na-ion batteries

• Yuko Matsukawa,
• Fabian Linsenmann,
• Maximilian A. Plass,
• George Hasegawa,
• Katsuro Hayashi and
• Tim-Patrick Fellinger

Beilstein J. Nanotechnol. 2020, 11, 1217–1229, doi:10.3762/bjnano.11.106

• originating from adsorption inside micropores. Herein, two different types of HCs prepared with different procedures are compared regarding their morphological characteristics as well as their electrochemical properties. Six samples were prepared via hydrothermal carbonization (HT) followed by pyrolytic

• the hydrothermal carbonization of saccharides [30][31]. Despite the slightly different preparation protocols, morphological differences between the hydrothermally obtained HCs are not significant (Figure 1). The two RF carbon samples showed well-defined monolithic macrostructures obtained by spinodal

• by the secondary catalytic effect of borax during the hydrothermal carbonization of sugars [32]. Gas sorption porosimetry of hard carbons N2 sorption porosimetry of the HT samples turned out to be problematic, since the equilibrium conditions were not reached (exemplarily shown in Supporting

Soybean-derived blue photoluminescent carbon dots

• Shanshan Wang,
• Wei Sun,
• Dong-sheng Yang and
• Fuqian Yang

Beilstein J. Nanotechnol. 2020, 11, 606–619, doi:10.3762/bjnano.11.48

• residuals to synthesize carbon nanoparticles by hydrothermal carbonization (HTC), annealing at high temperature, and laser ablation (LA) in a NH4OH solution. The carbon nanoparticles synthesized with the HTC process (HTC-CDs) exhibit photoluminescent characteristics with strong blue emission. The annealing

• luminescence properties. Hydrothermal carbonization (HTC), which can be considered as a “green technology”, has been used to produce photoluminescent CDs from biomass, including glucose, sucrose, citric acid [19], chitosan [20], orange juice [21], grass [22] and soy milk [10]. For example, Sahu et al. [21

• producing biocompatible CDs from biomass and biowaste and manipulating their PL characteristics. It is worth mentioning that we [33] previously studied the electrochemical performance of carbon particles of micrometer size, which were synthesized from the soybean residuals via hydrothermal carbonization and

Synthesis of amorphous and graphitized porous nitrogen-doped carbon spheres as oxygen reduction reaction catalysts

• Maximilian Wassner,
• Markus Eckardt,
• Andreas Reyer,
• Thomas Diemant,
• Michael S. Elsaesser,
• R. Jürgen Behm and
• Nicola Hüsing

Beilstein J. Nanotechnol. 2020, 11, 1–15, doi:10.3762/bjnano.11.1

• microporosity of the materials is critical for an efficient ORR. Keywords: amorphous carbon; graphitized carbon; hydrothermal carbonization; nitridation; nitrogen doping; oxygen reduction reaction (ORR); porosity; Introduction Fuel cells and metal–air batteries are important renewable energy technologies

• amorphous N-doped carbon spheres (NCSs) and graphitized N-doped carbon spheres (g-NCSs) by hydrothermal carbonization (HTC) of a glucose solution yielding carbon spheres that are either directly nitrided with ammonia or graphitized and then nitrided (nitrogen atoms in the graphitic lattice are given in blue

Glucose-derived carbon materials with tailored properties as electrocatalysts for the oxygen reduction reaction

• Rafael Gomes Morais,
• Natalia Rey-Raap,
• José Luís Figueiredo and
• Manuel Fernando Ribeiro Pereira

Beilstein J. Nanotechnol. 2019, 10, 1089–1102, doi:10.3762/bjnano.10.109

• -doped biomass-derived carbon materials were prepared by hydrothermal carbonization of glucose, and their textural and chemical properties were subsequently tailored to achieve materials with enhanced electrochemical performance towards the oxygen reduction reaction. Carbonization and physical activation

• to be an attractive alternative. In this context, hydrothermal carbonization (HTC) has appeared in recent years as an interesting strategy to obtain biomass-derived carbons due to its low cost and mild synthesis conditions, making the process environmentally friendly [34]. However, the main drawback

• contains nitrogen in its constitution [11][37], and by in situ methods in which nitrogen precursors are introduced during the hydrothermal carbonization [38]. An additional strategy that can be applied to biomass processing is ball milling, which has been proposed as a green, cheap and easy method to

Hydrothermal-derived carbon as a stabilizing matrix for improved cycling performance of silicon-based anodes for lithium-ion full cells

• Mirco Ruttert,
• Florian Holtstiege,
• Jessica Hüsker,
• Markus Börner,
• Martin Winter and
• Tobias Placke

Beilstein J. Nanotechnol. 2018, 9, 2381–2395, doi:10.3762/bjnano.9.223

• ] showed that Si nanoparticles (Si-NPs) can be embedded in spherical hydrothermal carbon via a simple one-step hydrothermal process and Hu et al. [53] used hydrothermal carbonization to form a thin carbon and SiOx layer around Si-NPs and reported a great improvement in cycling stability compared to pure Si

Sugarcane juice derived carbon dot–graphitic carbon nitride composites for bisphenol A degradation under sunlight irradiation

• Lan Ching Sim,
• Jing Lin Wong,
• Chen Hong Hak,
• Jun Yan Tai,
• Kah Hon Leong and
• Pichiah Saravanan

Beilstein J. Nanotechnol. 2018, 9, 353–363, doi:10.3762/bjnano.9.35

• -driven photocatalysis. Prasannan and Imae reported a simple and facile one-pot synthesis of fluorescent CDs from orange waste peels using the hydrothermal carbonization method. As prepared CDs were combined with zinc oxide (ZnO) to degrade naphthol blue–black azo dye under UV irradiation, and the

Fundamental properties of high-quality carbon nanofoam: from low to high density

• Natalie Frese,
• Shelby Taylor Mitchell,
• Christof Neumann,
• Amanda Bowers,
• Armin Gölzhäuser and
• Klaus Sattler

Beilstein J. Nanotechnol. 2016, 7, 2065–2073, doi:10.3762/bjnano.7.197

• and a stronger sp3-type electronic contribution, related to the inclusion of sp3 connections in their surface network. Keywords: carbon nanofoam; helium ion microscopy; hydrothermal carbonization; nanocarbons; Introduction Nanofoams are of considerable current interest due to their unique structure

• [23] with potential application in high energy density electrochemical supercapacitors. A promising formation method for high-quality carbon nanofoam is the low-temperature hydrothermal carbonization of sucrose [24]. In order to produce advanced carbon nanomaterials, there is a need for further

• help to better understand the hydrothermal carbonization process, and in addition, to tune the growth toward particular materials structures. Such studies can considerably expand the possibility of production of nanomaterials by hydrothermal carbonization. In this paper, we probe two carbon nanofoam